Zoznam zariadení

Ak s nami chcete spolupracovať, alebo potrebujete naše odborné znalosti pri analýze vašich vzoriek a/alebo pri interpretácii vašich výsledkov, nasledujúci zoznam zariadení vám poskytne predstavu o vedeckej práci vykonávanej na Katedre anorganickej chémie:

 

High-Performance Liquid Chromatography

  • HPLC (Merck) equipped with autosampler (AS-2000), intelligent pump (L-6200A), UV-VIS detector (L-4250) and fluorescence spectrophotometer (F-1050). The analytical software is ChromNav from Jasco.

Rq: currently, the installed column is a C18 column (Hypersil Gold – Thermo Fisher Scientific) and the solvents are water, methanol and acetonitrile.

 

contact: Olivier Monfort (monfort1uniba.sk)

 

Total Organic Carbon Analyzer

  • TOC-5000A (Shimadzu) for analysis of dissolved carbon in aqueous solutions.

 

contact: Olivier Monfort (monfort1uniba.sk)

 

Photoreactors 

  • Foto-Sihor (homemade box photoreactor) equipped with 2 to 4 lamps: either UVA (Sylvania BL368-15W with 5 µW/cm² UVA and 35 µW/cm² total at 1 m distance) or UVA-UVB (Sylvania Reptistar with 30% UVA and 5% UVB). 

  • Vertical tubular photoreactor equipped with 3 and 6 lamps: either UVA (Sylvania BL368-15W with 5 µW/cm² UVA and 35 µW/cm² total at 1 m distance) or UVA-UVB (Sylvania Reptistar with 30% UVA and 5% UVB).

  • UVA irradiation with 1.5 mW/cm² in the range 335-380 nm at 12 cm.

  • UVA irradiation with 3.5 mW/cm² in the range 335-380 nm at 12 cm.

Rq: Cut-off filters (350 nm, 400 nm and 430 nm) can be integrated to the above-mentionned photoreactors.

 

contact: Olivier Monfort (monfort1uniba.sk)

 

Anodization setup – DC power supply

  • LAB/SMS 3100 (ET system) with a voltage range 0-100 V and current density up to 30 A.

  • 2260B-250-4 360W (Keithley – Tektronix company) with multi-range voltage and current density

  • NPS1003D (WanpTek) with voltage range 0-100 V and current density up to 3 A.

 

contact: Martin Motola (martin.motola@uniba.sk)

 

Hydrothermal reactors – Stainless Steel Autoclaves

  • HTC230-V-100 (COL-INT-TECH) for max. P = 15 MPa and max. T = 200 °C.

  • HTC230-V-2 (COL-INT-TECH) for max. P = 15 MPa and max. T = 200 °C.

Rq: The reactors are equipped with Teflon chambers.

 

contact: Olivier Monfort (monfort1uniba.sk)

 

Spin-Coater

  • E461 (Ossila) for deposition of sol-gel precursors.

     

 contact: Olivier Monfort (monfort1uniba.sk)

 

Mufle furnaces

  • LE 05/11 (LAC) with Ht40P regulator for heating up to 1100 °C

  • 3013L (CLASIC) with integrated regulator for heating up to 1300 °C

  • 1313L (CLASIC) with integrated regulator for heating up to 1250 °C

 

contact: Olivier Monfort (monfort1uniba.sk)

 

Tube furnace

  •  4013T (CLASIC) with CLARE 4.0 regulator for heating up to 1300 °C under either air, N2 or Ar atmosphere.

     

 contact: Olivier Monfort (monfort1uniba.sk)

 

Ultrasonic probe

  • UZD 300 (Person) with a power of 300 W and frequency of 20 kHz.

     

 contact: Olivier Monfort (monfort1uniba.sk)

 

Centrifugation

  • EBA 20 S (Hettich) until 8000 rpm.

     

contact: Olivier Monfort (monfort1uniba.sk)